So what I said in the comment still holds: it could work (particularly in combination with a Dean-Stark apparatus to remove excess water but there is no way to know for sure unless someone tries it out. Under reflux while 35.5 grams (0.25 mole) of methyl iodide in 140 ml. of anhydrous. I was trying to determine whether I could synthesize methyl iodide by combining methanol, potassium iodide and sulphuric acid together. Methyl iodide, also called iodomethane, and commonly abbreviated MeI, is the chemical. It is used in organic synthesis as a source of methyl groups. Methyl. Phosphorous acid does not act as nucleophile and so the problem of a competing backward reaction, which you would have in your proposed synthesis, is largely prevented. I'd also like to add some caution: the reaction described in Organic Syntheses is not suited for beginners or in amateur setting.
Used in a one-pot Wittig synthesis of p Cstyrene. Tor Kihlberg, Per Gullberg and. The synthesis was performed by using llCmethyl iodide.
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